白及粉末饮片质量评价方法初步研究

doi:10.3976/j.issn.1002-4026.2017.03.006

Abstract

Abstract:

To establish the quality evaluation method of Bletilla striata powder, ten batches of samples from different areas were adapted to analysis. The identification method based on thin layer chromatogram (TLC) was improved, while the method with anthronesulfuric acid coloration was established to determine the polysaccharide in Bletilla striata powder. Meanwhile, the contents of microscopic, moisture, total ash, and acid insoluble ash in Bletilla striata powder had been studied and summarized. This method is convenient and stable so that it can be effectively and scientifically used for the quality evaluation of Bletilla striata powder.

Key words: powder, quality evaluation, Bletilla striata, polysaccharide

CLC Number:

R284. 1

WANG Tao, WANG Xiao-hui, CHEN Yan-nan, YANG Fan, ZHANG Chong, WANG Xiao. Preliminary study on the quality evaluation of Bletilla striata powder[J].SHANDONG SCIENCE, 2017, 30(3): 26-32.

References

［1］MABBERLEY D J. The PlantBook: A Portable Dictionary of the Vascular Plants ［M］.London: Cambridge University Press, 1997.
［2］张龙霏，胡晶红，张永清. 白及药理研究进展［J］.中国现代中药，2014, 16(1):8386.
［3］国家药典委员会. 中华人民共和国药典2015年版四部［M］.北京: 中国医药科技出版社，2015.
［4］赵菲菲，杨馨，徐丹，等．白及非多糖组分的止血作用及其机制的初步研究［J］.中国药理学通报，2016, 32(8): 11211126.
［5］汤逸飞，阮川芬，应晨，等．白及属植物化学成分与药理作用研究进展［J］.中草药，2014, 45(19): 28642872.
［6］孙爱静，庞素秋，王国权．中药白及化学成分与药理活性研究进展［J］.环球中医药，2016, 9(4): 507511.
［7］孙爱静，庞素秋，王国权．白及化学成分的分离及其抗肿瘤活性［J］.中国医药工业杂志，2016, 47(1): 3538.
［8］孙爱静，庞素秋，王国权．白及化学成分与抗肿瘤活性研究［J］.中国药学杂志，2016, 51(2):101104.
［9］王晓敏，吴明开，罗晓青．珍稀药用兰科植物白芨的研究现状与展望［J］.贵州农业科学，2011, 39(3):4245.
［10］李伟平，何良艳，丁志山．白及的应用及资源现状［J］.中华中医药学刊，2012, 30(1):158160.
［11］刘芳，傅超美，李小红，等．中药粉末饮片的研究与应用进展分析［J］.中国实验方剂学杂志，2016, 22(2):222225.
［12］湖南省食品药品监督管理局.湖南省中药饮片炮制规范（2010年版）［M］.长沙：湖南科学技术出版社，2010.
［13］国家药典委员会. 中华人民共和国药典中药材显微鉴别彩色图鉴［M］.北京: 人民卫生出版社，2009.
［14］杨毅，艾萍，杨丽萍，等．白及薄层色谱条件的改进和主要色谱斑点化学成分的鉴定［J］.亚太传统医药，2009, 5(9):2325.
［15］杨顺丽，杨枝中，李龙，等．白及薄层色谱鉴别方法的改进和高效液相指纹图谱研究［J］.云南中医学院学报，2015, 38(5):4145.
［16］王爱民，王永林，郑林，等．白及药材中多糖的含量测定［J］.中国中药杂志，2009, 34(22):29632965.
［17］陶平德，常明泉，李德福，等．蒽酮硫酸法测定复方白及乳膏中白及多糖的含量［J］.儿科药学杂志，2012, 18(9):4043.
［18］秦亚东，汪荣斌，周宙．不同产地白及多糖含量测定［J］.安徽科技学院学报，2014, 28(3):4144.
［19］朱海涛，楚亚琴，陈黎．正交试验优选蒽酮硫酸法测定白芨多糖含量条件［J］.中国医院药学杂志，2014, 34(20):17141718.
［20］吴凤云，邱丽莎，崔秀明，等．白及品质特征影响因素研究［J］.中国医院药学杂志，2016, 36(21):18381844.
［21］石上梅，钱忠直．逐步建立和完善提高符合中医药特点的中药质量标准——解读《中国药典》2010年版(一部)［J］.中国现代中药，2010, 12 (9):36.

[1]	YANG Zhicheng, SUN Caihong, YE Guan. Quality evaluation of Ganoderma lucidum as a medicinal material based on polysaccharides and entropy-weighted TOPSIS [J]. Shandong Science, 2024, 37(6): 31-41.
[2]	ZENG Ting, YANG Ran, LI Qingjun, GONG Yanan, WANG Shuzhen, LIU Qian. Effects of Dioscorea opposita Thunb. polysacchariades on exercise-related fatigue in mice through the PI3K/AKT/Gsk-3β pathway [J]. Shandong Science, 2024, 37(6): 51-58.
[3]	HUANG Jing, BAI Zhihao, WU Ke, DU Lixin, ZHANG Ruiyun, LI Hong, HUANG Liqian. Properties of radiative-cooling nylon filaments and their knitted fabrics [J]. Shandong Science, 2024, 37(4): 65-74.
[4]	MIAO Xuzhong, LI Xiufen, GAO Yanyan, ZHANG Xue, ZHANG Xiqing, QIAO Luqin. Optimization of preparation of persimmon peel polysaccharide chromium using response surface methodology [J]. Shandong Science, 2024, 37(2): 127-134.
[5]	WU Yonghao, XIE Hebing, HOU Hairong, WANG Rongchun, CHEN Xiqiang. Protective effect of Feirepuqing Powder on hypoxia-induced sports injury in zebrafish model by inhibiting Hif1α [J]. Shandong Science, 2024, 37(1): 32-38.
[6]	ZHANG Hui-min, SONG Jian, XU Lin, DONG Xue, ZHONG Fang-xiao. Improvement of the TLC identification standard of Yinqiao Powder in Chinese Pharmacopoeia [J]. Shandong Science, 2022, 35(4): 9-14.
[7]	CHEN Jian-wei,LIU Shuai,MA Jian,GUO Rui,SONG Jiang-feng,BAI Xue,ZOU Long-sen,SU Yi-fan. High-performance coil backplane for electromagnetic ultrasonic sensor and its optimization design [J]. Shandong Science, 2022, 35(2): 70-78.
[8]	Ming MEI,Jin ZHOU,Yi ZHANG,Liang-peng MA,Ming YANG,Song HU. Isolation and purification of polysaccharide from Smilacis Chinae Rhizoma [J]. Shandong Science, 2021, 34(6): 1-8.
[9]	YI Sai-ni, ZHANG Wen-jiao, LI Liang-yuan, XIAO Cheng-hong, TANG Xin, LIU Qin, SU Da-peng, XU Chun-yun, Zhang Jin-qiang, ZHOU Tao. The inhibition of loganin on microglia activation [J]. Shandong Science, 2021, 34(5): 34-41.
[10]	ZHOU Xin-pei, CHEN Wei, HE Yan. Numerical study of the flue gas desulfurization system using rapid preparation amorphous powder activated coke as desulfurizer [J]. Shandong Science, 2021, 34(5): 86-96.
[11]	ZOU Hong-yuan, ZHU Cheng-yue, ZHANG Shan-shan, KONG Rui-qi, ZHANG Yun, LIU Ke-chun. Protective effect of peony seed oil microcapsule powder on isoniazid-induced developmental toxicity in zebrafish [J]. Shandong Science, 2021, 34(4): 45-51.
[12]	LI Ling-yu, LI Yu-chen, ZUO Zhao-he, TIAN bao-lan, ZHENG Zhen-jia. Development of high performance gel chromatography for the determination of inulin polymerization [J]. Shandong Science, 2020, 33(4): 1-6.
[13]	LU De-peng, LÜ Yan, WANG Xiao-di, TONG Su-mei, LI Ji-shun, HU Jin-dong. Control efficacy of Trichoderma wettable powder on tomato Fusarium wilt [J]. Shandong Science, 2020, 33(2): 22-26.
[14]	CHEN Yan-fei, SONG Xiao-cun, LAI Hua-sheng, WEN Xiao-qiang, ZHOU Ji-xue. Fracture failure analysis and process improvement of iron-based powder metallurgy gears [J]. Shandong Science, 2020, 33(2): 27-32.
[15]	CHENG Ke-qing, WANG Chong-xu, XU Tong, LIN Ying, ZHOU Jie, DONG Peng, LI Li-ming, YU Jing-ping. Research progress on quality assessment of Panacis Quinquefolii Radix [J]. SHANDONG SCIENCE, 2018, 31(4): 39-43.

Preliminary study on the quality evaluation of Bletilla striata powder

PDF (PC)

Like

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Metrics

Comments

Recommended 0