J4 ›› 2012, Vol. 25 ›› Issue (2): 26-29.doi: 10.3976/j.issn.1002-4026.2012.02.006

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Identification of  Glehnia littoralis  by 13CNMR fingerprint

 LIU Jing, Dan Staerk*, SUN Qing-Lei, LI En-Xia, ZHAO Mei, MA Guang-Cun, JIANG Ting, LV Rui-Min   

  1. 1.Shandong Analysis and Test Center, Shandong Academy of Sciences, Jinan 250014, China; 2.Department of Basic Sciences and Environment,Faculty,of Life Sciences,University of Copenhagen,Thorvaldsensvej 40,DK 1871,Denmark
  • Received:2011-10-18 Online:2012-04-20 Published:2012-04-20

Abstract:

      We employed a universial extract approach to obtain Glehnia littoralis extracts reflecting the their total characteristics. We further applied a Fourier transform nuclear magnetic resonance spectrometer to determine the Carbon-13  Nuclear Magnetic Resonance (13CNMR) fingerprints of different Glehnia littoralis extracts and calculated their similarities with vectorial angle method. Results show that the resonant peaks of many components exist in the fingerprints of different Glehnia littoralis extracts. The characteristic resonant peaks of their active components exhibit better repeatability and characteristics. A joint analysis of 13CNMR fingerprints and their characteristic peaks would provide an identification basis for Glehnia littoralis.

Key words: 13CNMR, fingerprint, Glehnia littoralis, identification

CLC Number: 

  • O697.61