J4 ›› 2010, Vol. 23 ›› Issue (6): 44-47.

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Comparisons of Two Methods for Extraction and Determination of Chlorpyrifos in Water

 WEI Yan-Li1, ZHANG Xin-Jian1, LI Ji-Shun1, XU Xin-Hua2, LI hong-Mei1, YANG He-Tong1   

  1. 1.Shandong Provincial Key Laboratory of Applied Microbiology, Biotechnology Center of Shandong Academy of Sciences, Jinan 250014, China; 2. Shandong Sinoagri Union Biotechnology Co., Ltd.,Jinan 250014, China
  • Received:2010-06-25 Online:2010-12-20 Published:2010-12-20

Abstract:

         We compared two different extraction and determination approaches of chlorpyrifos in water. The approach of petroleum ether extraction and UV spectrophotometer determination is simpler and quicker, so it can be employed for initial screening of massive samples. The approach of ethyl acetate extraction and HPLC determination has higher precision than the former approach, but it is timeconsuming and laborious, so it is suitable for the accurate determination of a small quantity of samples. The minimum detectable concentrations of these two approaches are 0.1 mg·L-1 and 0.02 mg·L-1, respectively.

Key words: chlorpyrifos, extraction, determination

CLC Number: 

  • S481+.8