J4 ›› 2011, Vol. 24 ›› Issue (3): 83-86.

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Preparation of Celery Spices

 JI Wen-Hua, GAO Gan-Shan   

  1. Shandong Analysis and Test Center, Jinan 250014, China
  • Received:2011-01-06 Online:2011-06-20 Published:2011-06-20

Abstract:

       This paper addressed preparation methods of dihydrocarvone, dihydrocarveol and dihydrocarvyl acetate with carvone as raw material and such steps as reduction, esterification, especially the ZnROH reduction. We employed NMR and ESIMS to determine the structures of these objective compounds. This synthesis process has such positives as low cost and high recovery rate (more than 80%), and has some references to industrial production.

Key words: carvone, spice, synthesis