SHANDONG SCIENCE ›› 2017, Vol. 30 ›› Issue (5): 14-20.doi: 10.3976/j.issn.1002-4026.2017.05.003

• Traditional Chinese medicine and natural active products • Previous Articles     Next Articles

Determination of 35 elements in Chinese caterpillar fungus from Qinghai and Tibet by microwave digestionICP-MS

ZHANG Min-min1,ZHAO Heng-qiang1,ZHAO Zhi-guo1,LIU Wei1,LIU Qian1,LIANG Yan1,GENG Yan-ling1,HUANG Lu-qi2,WANG Xiao1*   

  1. 1.Shandong Provincial Key Laboratory Breeding Base of TCM Quality Control Technology, Process Control Research Center of Traditional Chinese Medicine of Shandong Academy of Sciences, Shandong Analysis and Test Center,  Jinan 250014, China; 2.National Resource Chinese Center for Materia Medica, Key Laboratory of Road to  the Cultivation of Chinese Medicine ,China Academy of Chinese Medical Sciences, Beijing 100700,China
  • Received:2017-05-10 Online:2017-10-20 Published:2017-10-20

Abstract:

To determine the contents of 35 elements (including 16 rare earth elements) in 17 batches of Chinese caterpillar fungus from Qinghai and Tibet and make preliminary identification analysis of their habitats, a total of 35 elements in Chinese caterpillar fungus samples were determined by microwave digestionICPMS, including 3 batches from Yushu, 4 batches from Naqu and 10 batches from Guoluo. Furthermore, cluster analysis was carried out on the measurement results of 3 producing areas. Results showed that the contents of 35 elements in 17 kinds of Chinese caterpillar fungus samples from different origins have obvious differences. And the limits of the 4 kinds of harmful elements (Cd, Pb, As and Cu) were recommended. The results of cluster analysis showed that the samples from Yushu and Guoluo were close, and the difference was small, while the sample from Naqu was far away, and its relative difference was larger. This method is quick, accurate and feasible, which provides a theoretical basis for quality control and medication guidance of Chinese caterpillar fungus from different habitats.

Key words: ICP-MS, rare earth elements, Chinese caterpillar fungus, trace elements

CLC Number: 

  • R284.1