大孔树脂层析-酸性氧化铝吸附法制备蛇床子素工艺研究

doi:10.3976/j.issn.1002-4026.2014.04.007

SHANDONG SCIENCE ›› 2014, Vol. 27 ›› Issue (4): 38-41.doi: 10.3976/j.issn.1002-4026.2014.04.007

• Traditional Chinese medicine and natural active products • Previous Articles Next Articles

Osthole preparation based on macroporus resin column chromatography and acidic alumina absorption

SUN Shi-Qing, SHI Jian-Guo, MA Yao-Hong, YANG Jun-Hui

Received:2014-03-13 Published:2014-08-20 Online:2014-08-20

Abstract

Abstract:

We optimized extraction and separation conditions of osthole with L₉(3⁴) orthogonal design and osthole obtaining rate and osthole content in preparation as main indexes. Results show that ethanol concentration has great impact on osthole obtaining rate. It is the highest with 95% ethanol to extract raw powder of common cnidium fruit, acidic aluminum absorption and macroporus resin column chromatography.

Key words: common cnidium fruit, macroporus resin, orthogonal experiment, osthole

CLC Number:

R284.2

SUN Shi-Qing, SHI Jian-Guo, MA Yao-Hong, YANG Jun-Hui. Osthole preparation based on macroporus resin column chromatography and acidic alumina absorption[J].SHANDONG SCIENCE, 2014, 27(4): 38-41.

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Open Access This article is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License (CC BY-NC 4.0), which permits third parties to freely share (i.e., copy and redistribute the material in any medium or format) and adapt (i.e., remix, transform, or build upon the material) the articles published in this journal, provided that appropriate credit is given, a link to the license is provided, and any changes made are indicated. The material may not be used for commercial purposes. For details of the CC BY-NC 4.0 license, please visit: https://creativecommons.org/licenses/by-nc/4.0

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Osthole preparation based on macroporus resin column chromatography and acidic alumina absorption

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