黑色签字笔,种类区分,">溶剂," /> 黑色签字笔,种类区分,">溶剂,"/> black signature pen,"/> <span style="font-size: 10.5pt;">GC-MS based solvent component detection in black signature pen</span>

SHANDONG SCIENCE ›› 2016, Vol. 29 ›› Issue (3): 92-96.doi: 10.3976/j.issn.1002-4026.2016.03.016

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GC-MS based solvent component detection in black signature pen

CHEN Yue 1 , LIU Wei2, ZOU Ji-xin 3   

  1. 1.Shandong Analysis and Test Center, Jinan 250014, China; 2. Shandong University of Political Science and Law,Jinan 250014, China; 3. Institute of Forensic Science, Ministry of Public Security, Beijing 100038, China
  • Received:2015-07-01 Online:2016-06-20 Published:2016-06-20

Abstract:

We detected solvent component in 24 kinds of black signature pens with GC-MS. We extracted solvent component in black signature pen with methanol as extraction solvent. Results show that 1, 2-propanediol and phenoxyethanol are the most common solvents in black signature pen. Distinction rate is about 50% for the 24 kinds of samples. We further studied the variation rule of 1, 2-propanediol in a short time. 1, 2-propanediol changed to the maximum on the first day of handwriting formation. The variation tends to be stable on the fifth day. The
research provides important evidence for the identification of handwriting formation time.

Key words: solvent, category distinction, black signature pen')">black signature pen

CLC Number: 

  • Cite this article

    CHEN Yue1,LIU Wei, ZOU Ji-xin. GC-MS based solvent component detection in black signature pen[J].SHANDONG SCIENCE, 2016, 29(3): 92-96.