黑色签字笔,种类区分,">溶剂," /> 黑色签字笔,种类区分,">溶剂,"/> black signature pen,"/> <span style="font-size: 10.5pt;">气质联用法检验签字笔字迹中溶剂成分</span>

山东科学 ›› 2016, Vol. 29 ›› Issue (3): 92-96.doi: 10.3976/j.issn.1002-4026.2016.03.016

• 其他研究论文 • 上一篇    下一篇

气质联用法检验签字笔字迹中溶剂成分

陈跃1,刘伟2,邹积鑫3   

  1. 1.山东省分析测试中心,山东济南250014;2.山东政法学院,山东济南250014;3.公安部物证鉴定中心,北京100038
  • 收稿日期:2015-07-01 出版日期:2016-06-20 发布日期:2016-06-20
  • 作者简介:陈跃(1983-),男,助理研究员,博士研究生,研究方向为分析技术?Email:chenyue2006@126.com
  • 基金资助:

    山东省高校证据鉴识重点实验室开放课题(KFKT(SUPL).201413)

GC-MS based solvent component detection in black signature pen

CHEN Yue 1 , LIU Wei2, ZOU Ji-xin 3   

  1. 1.Shandong Analysis and Test Center, Jinan 250014, China; 2. Shandong University of Political Science and Law,Jinan 250014, China; 3. Institute of Forensic Science, Ministry of Public Security, Beijing 100038, China
  • Received:2015-07-01 Online:2016-06-20 Published:2016-06-20

摘要:

采用气质联用法检测了24种黑色签字笔中的溶剂成分?采用甲醇为提取溶剂,对黑色签字笔字迹中的溶剂成分进行了提取?结果表明,1,2丙二醇和苯氧乙醇是黑色签字笔中最常见的溶剂,检测的24种样品区分率在50%左右?对1,2-丙二醇在短时间内的变化规律进行了研究,样品中1,2-丙二醇在笔迹形成后第1天变化最大,到第5天后变化趋于稳定?该研究为鉴定字迹的形成时间提供了重要的依据?

关键词: 黑色签字笔')">">黑色签字笔, 种类区分')">">种类区分, 溶剂')">">溶剂

Abstract:

We detected solvent component in 24 kinds of black signature pens with GC-MS. We extracted solvent component in black signature pen with methanol as extraction solvent. Results show that 1, 2-propanediol and phenoxyethanol are the most common solvents in black signature pen. Distinction rate is about 50% for the 24 kinds of samples. We further studied the variation rule of 1, 2-propanediol in a short time. 1, 2-propanediol changed to the maximum on the first day of handwriting formation. The variation tends to be stable on the fifth day. The
research provides important evidence for the identification of handwriting formation time.

Key words: solvent, category distinction, black signature pen')">black signature pen

中图分类号: 

  • 引用本文

    陈跃,刘伟,邹积鑫. 气质联用法检验签字笔字迹中溶剂成分[J]. 山东科学, 2016, 29(3): 92-96.

    CHEN Yue1,LIU Wei, ZOU Ji-xin. GC-MS based solvent component detection in black signature pen[J]. SHANDONG SCIENCE, 2016, 29(3): 92-96.